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For GCMS analysis 1 l of the sample (45 replicates) was injected with a split ratio of 20:1 on a Famewax, 30 m x 0.25 mm iD, 0.25 m df capillary column (Restek, Bad Homburg)

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doi:10.1016/S0753-3322(03)00043-X 21