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As some of the drugs were banned in some EU states but not others, new law enforcement problems arose until a European-wide "joint action" on new synthetic drugs was developed in 1997 and expanded in 2005

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Intra-day (within-run) accuracy and precision were determined by taking the largest percent coefficient of variation (%CV) and most extreme accuracies for each control concentration out of each of the three runs ( n = 6)

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